Information card for entry 7702557

Structure parameters

• Formula: C30 H46.3 Cl4 N15 Ni2 O22.65
• Calculated formula: C30 H42.15 Cl4 N15 Ni2 O22.65
• Title of publication: N‒N Bridged dinuclear complexes with Mn(ii), Ni(ii), Cu(ii), Zn(ii) and Cd(ii); examples with antiferromagnetic and ferromagnetic coupling
• Authors of publication: Xu, Zhiqiang; Thompson, Laurence K.; Black, Daniel A.; Ralph, Corbin; Miller, David O.; Leech, Michael A.; Howard, Judith A. K.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 13
• Pages of publication: 2042
• a: 19.277 ± 0.005 Å
• b: 21.233 ± 0.005 Å
• c: 12.479 ± 0.003 Å
• α: 90°
• β: 98.2 ± 0.02°
• γ: 90°
• Cell volume: 5056 ± 2 ų
• Cell temperature: 299.2 K
• Ambient diffraction temperature: 299.2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1462
• Residual factor for significantly intense reflections: 0.11
• Weighted residual factors for all reflections: 0.113
• Weighted residual factors for all reflections included in the refinement: 0.112
• Goodness-of-fit parameter for all reflections: 4.734
• Goodness-of-fit parameter for all reflections included in the refinement: 5.57
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No