Information card for entry 7702592

Structure parameters

• Formula: C30 H32 N P Pd
• Calculated formula: C30 H26 N P Pd
• Title of publication: Palladium(ii) complexes with the bidentate iminophosphine ligand [Ph2PCH2C(Ph)N(2,6-Me2C6H3)]
• Authors of publication: Coleman, Karl S.; Green, Malcolm L. H.; Pascu, Sofia I.; Rees, Nicholas H.; Cowley, A. R.; Rees, Leigh H.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 22
• Pages of publication: 3384
• a: 7.859 ± 0.0007 Å
• b: 9.2 ± 0.0013 Å
• c: 18.778 ± 0.003 Å
• α: 89.044 ± 0.006°
• β: 84.199 ± 0.008°
• γ: 70.296 ± 0.007°
• Cell volume: 1271.4 ± 0.3 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0868
• Weighted residual factors for all reflections included in the refinement: 0.0704
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1147
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No