Information card for entry 7702620

Structure parameters

• Common name: [{NiCl(IMmepy)}~2~(μ-Cl)~2~]
• Chemical name: Bis(μ-chloro)bis(chloro(2-(6'-methyl-2'-pyridyl)-4,4,5,5- tetramethylimidazoline-1-oxy)nickel(II))
• Formula: C13 H18 Cl2 N3 Ni O
• Calculated formula: C13 H18 Cl2 N3 Ni O
• Title of publication: Syntheses, structures, magnetic, and spectroscopic properties of cobalt(ii), nickel(ii) and zinc(ii) complexes containing 2-(6-methyl)pyridyl-substituted nitronyl and imino nitroxide†
• Authors of publication: Yamamoto, Youhei; Suzuki, Takayoshi; Kaizaki, Sumio
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2001
• Journal issue: 19
• Pages of publication: 2943
• a: 10.2119 ± 0.0019 Å
• b: 10.892 ± 0.003 Å
• c: 14.5148 ± 0.0017 Å
• α: 90°
• β: 99.292 ± 0.011°
• γ: 90°
• Cell volume: 1593.3 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0563
• Residual factor for significantly intense reflections: 0.03
• Weighted residual factors for significantly intense reflections: 0.0759
• Weighted residual factors for all reflections included in the refinement: 0.0847
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No