Crystallography Open Database

Information card for entry 7702689

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Coordinates	7702689.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H55 Cl O3 P2 Ru
Calculated formula	C33 H54 Cl O3 P2 Ru
Title of publication	A series of ruthenium(ii) complexes containing the bulky, functionalized trialkylphosphines tBu2PCH2XC6H5 as ligands
Authors of publication	Jung, Stefan; Ilg, Kerstin; Brandt, Carsten D.; Wolf, Justin; Werner, Helmut
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2002
Journal issue	3
Pages of publication	318
a	11.676 ± 0.002 Å
b	12.255 ± 0.003 Å
c	13.537 ± 0.003 Å
α	79.57 ± 0.03°
β	68.26 ± 0.03°
γ	82.44 ± 0.03°
Cell volume	1765.1 ± 0.8 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0699
Residual factor for significantly intense reflections	0.0509
Weighted residual factors for significantly intense reflections	0.1398
Weighted residual factors for all reflections included in the refinement	0.1464
Goodness-of-fit parameter for all reflections included in the refinement	0.947
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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