Information card for entry 7702702

Structure parameters

• Formula: C24 H14 F13 O P
• Calculated formula: C24 H14 F13 O P
• Title of publication: Synthesis and coordination chemistry of ortho-perfluoroalkyl-derivatised triarylphosphines
• Authors of publication: Croxtall, Ben; Fawcett, John; Hope, Eric G.; Stuart, Alison M.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 4
• Pages of publication: 491
• a: 10.9421 ± 0.0011 Å
• b: 10.0232 ± 0.001 Å
• c: 42.863 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4701 ± 0.8 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0585
• Residual factor for significantly intense reflections: 0.0513
• Weighted residual factors for significantly intense reflections: 0.1531
• Weighted residual factors for all reflections included in the refinement: 0.1573
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No