Information card for entry 7702707

Structure parameters

• Formula: C39 H28 Cl F6 O P2 Rh
• Calculated formula: C39 H28 Cl F6 O P2 Rh
• Title of publication: Synthesis and coordination chemistry of ortho-perfluoroalkyl-derivatised triarylphosphines
• Authors of publication: Croxtall, Ben; Fawcett, John; Hope, Eric G.; Stuart, Alison M.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 4
• Pages of publication: 491
• a: 11.4686 ± 0.0011 Å
• b: 11.1852 ± 0.0011 Å
• c: 13.8374 ± 0.0014 Å
• α: 90°
• β: 101 ± 0.002°
• γ: 90°
• Cell volume: 1742.4 ± 0.3 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0336
• Residual factor for significantly intense reflections: 0.0302
• Weighted residual factors for significantly intense reflections: 0.072
• Weighted residual factors for all reflections included in the refinement: 0.0736
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No