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Information card for entry 7702758
Preview
Coordinates | 7702758.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C55 H95 Cs2 Li N6 O20 |
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Calculated formula | C55 H95 Cs2 Li N6 O20 |
Title of publication | Formation of [M(15-crown-5)2]2[Li(NHPy)3] (M = K or Cs): the first structurally authenticated examples of a monomeric lithium species coordinated by three amide anions |
Authors of publication | Liddle, Stephen T.; Clegg, William |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 2001 |
Journal issue | 24 |
Pages of publication | 3549 |
a | 14.2706 ± 0.0009 Å |
b | 14.6824 ± 0.0009 Å |
c | 18.2599 ± 0.0011 Å |
α | 77.781 ± 0.002° |
β | 71.818 ± 0.002° |
γ | 68.921 ± 0.002° |
Cell volume | 3370.3 ± 0.4 Å3 |
Cell temperature | 220 ± 2 K |
Ambient diffraction temperature | 220 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1194 |
Residual factor for significantly intense reflections | 0.0651 |
Weighted residual factors for significantly intense reflections | 0.182 |
Weighted residual factors for all reflections included in the refinement | 0.2108 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.884 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7702758.html
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