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Information card for entry 7702783
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Coordinates | 7702783.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C24 H54 O6 Si6 |
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Calculated formula | C24 H55 O6 Si6 |
Title of publication | Linking of metal centres through boryl ligands: synthesis, spectroscopic and structural characterisation of symmetrically bridged boryl complexes |
Authors of publication | Aldridge, Simon; Calder, Richard J.; Rossin, Andrea; Dickinson, Anthony A.; Willock, David J.; Jones, Cameron; Evans, David J.; Steed, Jonathan W.; Light, Mark E.; Coles, Simon J.; Hursthouse, Michael B. |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 2002 |
Journal issue | 9 |
Pages of publication | 2020 |
a | 18.52 ± 0.002 Å |
b | 17.898 ± 0.002 Å |
c | 12.451 ± 0.003 Å |
α | 90° |
β | 96 ± 0.02° |
γ | 90° |
Cell volume | 4104.5 ± 1.2 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 4 |
Space group number | 12 |
Hermann-Mauguin space group symbol | C 1 2/m 1 |
Hall space group symbol | -C 2y |
Residual factor for all reflections | 0.1033 |
Residual factor for significantly intense reflections | 0.0689 |
Weighted residual factors for significantly intense reflections | 0.2193 |
Weighted residual factors for all reflections included in the refinement | 0.2391 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.104 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7702783.html
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