Information card for entry 7702820

Structure parameters

• Formula: C46 H40 O7 P4
• Calculated formula: C46 H40 O7 P4
• Title of publication: Synthesis and structural characterisation of the first tris(diacylpnictido)phosphines, P[E{C(O)R}2]3, E = P or As, R = But or Ph
• Authors of publication: Jones, Cameron; Junk, Peter C.; Williams, Thomas C.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 12
• Pages of publication: 2417
• a: 12.93 ± 0.003 Å
• b: 14.012 ± 0.003 Å
• c: 14.939 ± 0.003 Å
• α: 97.21 ± 0.03°
• β: 112.28 ± 0.03°
• γ: 116.39 ± 0.03°
• Cell volume: 2097.6 ± 1.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0624
• Residual factor for significantly intense reflections: 0.0416
• Weighted residual factors for significantly intense reflections: 0.0877
• Weighted residual factors for all reflections included in the refinement: 0.0956
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No