Information card for entry 7702840

Structure parameters

• Formula: C21 H45 Cl3 P3 Re
• Calculated formula: C21 H28 Cl3 P3 Re
• Title of publication: Manganese and rhenium triphosphorus macrocycle complexes and reactions with alkenes
• Authors of publication: Baker, Robert J.; Edwards, Peter G.; Gracia-Mora, Jes??s; Ingold, Florent; Abdul Malik, K. M.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 21
• Pages of publication: 3985
• a: 14.409 ± 0.003 Å
• b: 15.947 ± 0.003 Å
• c: 11.737 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2696.9 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0677
• Residual factor for significantly intense reflections: 0.0641
• Weighted residual factors for significantly intense reflections: 0.1492
• Weighted residual factors for all reflections included in the refinement: 0.1508
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No