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Information card for entry 7702856
Preview
Coordinates | 7702856.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C88 H144 Ga2 K2 N4 O18 |
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Calculated formula | C88 H120 Ga2 K2 N4 O18 |
Title of publication | The reactivity of diazabutadienes toward low oxidation state Group 13 iodides and the synthesis of a new gallium(i) carbene analogue |
Authors of publication | Baker, Robert J.; Farley, Robert D.; Jones, Cameron; Kloth, Marc; Murphy, Damien M. |
Journal of publication | Journal of the Chemical Society, Dalton Transactions |
Year of publication | 2002 |
Journal issue | 20 |
Pages of publication | 3844 |
a | 20.844 ± 0.004 Å |
b | 26.08 ± 0.005 Å |
c | 17.719 ± 0.004 Å |
α | 90° |
β | 104.7 ± 0.03° |
γ | 90° |
Cell volume | 9317 ± 4 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1111 |
Residual factor for significantly intense reflections | 0.069 |
Weighted residual factors for significantly intense reflections | 0.1418 |
Weighted residual factors for all reflections included in the refinement | 0.1565 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.084 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7702856.html
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structural data.