Information card for entry 7702858

Structure parameters

• Formula: C64 H102 Ga2 K2 N4 O3
• Calculated formula: C64 H102 Ga2 K2 N4 O3
• Title of publication: The reactivity of diazabutadienes toward low oxidation state Group 13 iodides and the synthesis of a new gallium(i) carbene analogue
• Authors of publication: Baker, Robert J.; Farley, Robert D.; Jones, Cameron; Kloth, Marc; Murphy, Damien M.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 2002
• Journal issue: 20
• Pages of publication: 3844
• a: 12.559 ± 0.003 Å
• b: 12.623 ± 0.003 Å
• c: 12.931 ± 0.003 Å
• α: 67.45 ± 0.03°
• β: 77.15 ± 0.03°
• γ: 62.55 ± 0.03°
• Cell volume: 1677.5 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0567
• Residual factor for significantly intense reflections: 0.0425
• Weighted residual factors for significantly intense reflections: 0.0942
• Weighted residual factors for all reflections included in the refinement: 0.1003
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No