Information card for entry 7703040

Structure parameters

• Formula: C48 H81 Co5 N2 O18
• Calculated formula: C48 H81 Co5 N2 O18
• Title of publication: Structural characterization and magnetic property studies of a mixed-valence {Co^IIICo} complex with a μ₄-oxo tetrahedral {Co} motif.
• Authors of publication: Fiorini, Guillermo; Carrella, Luca; Rentschler, Eva; Alborés, Pablo
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 3
• Pages of publication: 932 - 940
• a: 12.4276 ± 0.0011 Å
• b: 24.0925 ± 0.0018 Å
• c: 22.4107 ± 0.0016 Å
• α: 90°
• β: 97.991 ± 0.007°
• γ: 90°
• Cell volume: 6644.9 ± 0.9 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1992
• Residual factor for significantly intense reflections: 0.0947
• Weighted residual factors for significantly intense reflections: 0.2268
• Weighted residual factors for all reflections included in the refinement: 0.3092
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No