Information card for entry 7703107

Structure parameters

• Formula: C25 H35 B Cl2 N O4 P
• Calculated formula: C25 H35 B Cl2 N O4 P
• Title of publication: Addition reactions and diazomethane capture by the intramolecular P-O-B FLP: tBu₂POBcat.
• Authors of publication: Zhu, Diya; Qu, Zheng-Wang; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 3
• Pages of publication: 901 - 910
• a: 8.4602 ± 0.0008 Å
• b: 8.5103 ± 0.0009 Å
• c: 18.4139 ± 0.0019 Å
• α: 83.507 ± 0.005°
• β: 85.826 ± 0.004°
• γ: 81.688 ± 0.004°
• Cell volume: 1301.3 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150.15 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0803
• Residual factor for significantly intense reflections: 0.0435
• Weighted residual factors for significantly intense reflections: 0.0856
• Weighted residual factors for all reflections included in the refinement: 0.0987
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0323
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No