Information card for entry 7703112

Structure parameters

• Formula: C21 H27 B N O4 P
• Calculated formula: C21 H27 B N O4 P
• Title of publication: Addition reactions and diazomethane capture by the intramolecular P-O-B FLP: tBu₂POBcat.
• Authors of publication: Zhu, Diya; Qu, Zheng-Wang; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 3
• Pages of publication: 901 - 910
• a: 12.434 ± 0.01 Å
• b: 12.992 ± 0.01 Å
• c: 14.929 ± 0.012 Å
• α: 69.501 ± 0.017°
• β: 87.98 ± 0.03°
• γ: 70.6 ± 0.04°
• Cell volume: 2122 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1093
• Residual factor for significantly intense reflections: 0.0514
• Weighted residual factors for significantly intense reflections: 0.0962
• Weighted residual factors for all reflections included in the refinement: 0.1155
• Goodness-of-fit parameter for all reflections included in the refinement: 0.994
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No