Information card for entry 7703177

Structure parameters

• Formula: C32 H15 F36 Li6 O15
• Calculated formula: C32 H15 F36 Li6 O15
• Title of publication: Facile synthesis of novel lithium β-diketonate glyme adducts: the effect of molecular engineering on the thermal properties.
• Authors of publication: Peddagopu, Nishant; Rossi, Patrizia; Bonaccorso, Carmela; Bartasyte, Ausrine; Paoli, Paola; Malandrino, Graziella
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 4
• Pages of publication: 1002 - 1006
• a: 17.93 ± 0.001 Å
• b: 9.2458 ± 0.0005 Å
• c: 30.375 ± 0.002 Å
• α: 90°
• β: 103.158 ± 0.003°
• γ: 90°
• Cell volume: 4903.3 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0722
• Residual factor for significantly intense reflections: 0.0605
• Weighted residual factors for significantly intense reflections: 0.1418
• Weighted residual factors for all reflections included in the refinement: 0.1561
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No