Information card for entry 7703262

Structure parameters

• Formula: C44 H30 B F20 Sb
• Calculated formula: C44 H30 B F20 Sb
• Title of publication: Diverse structure and reactivity of pentamethylcyclopentadienyl antimony(iii) cations.
• Authors of publication: Coughlin, Omar; Krämer, Tobias; Benjamin, Sophie L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 6
• Pages of publication: 1726 - 1730
• a: 12.4426 ± 0.0004 Å
• b: 12.7883 ± 0.0004 Å
• c: 15.2203 ± 0.0005 Å
• α: 108.476 ± 0.003°
• β: 104.868 ± 0.003°
• γ: 103.354 ± 0.003°
• Cell volume: 2087.32 ± 0.14 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0714
• Residual factor for significantly intense reflections: 0.0452
• Weighted residual factors for significantly intense reflections: 0.0853
• Weighted residual factors for all reflections included in the refinement: 0.0978
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No