Information card for entry 7703363

Structure parameters

• Formula: Ge4 O20.5 Rb6 U3
• Calculated formula: Ge4 O20.5 Rb6 U3
• Title of publication: Crystal growth of novel 3D skeleton uranyl germanium complexes: influence of synthetic conditions on crystal structures.
• Authors of publication: Li, Haijian; Kegler, Philip; Alekseev, Evgeny V.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 7
• Pages of publication: 2244 - 2257
• a: 7.4797 ± 0.0004 Å
• b: 9.9013 ± 0.0006 Å
• c: 10.1327 ± 0.0007 Å
• α: 70.179 ± 0.006°
• β: 89.046 ± 0.005°
• γ: 86.24 ± 0.005°
• Cell volume: 704.43 ± 0.08 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1119
• Residual factor for significantly intense reflections: 0.0591
• Weighted residual factors for significantly intense reflections: 0.1383
• Weighted residual factors for all reflections included in the refinement: 0.148
• Goodness-of-fit parameter for all reflections included in the refinement: 0.927
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No