Crystallography Open Database

Information card for entry 7703365

Preview

Coordinates	7703365.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Br F Ge4 K8 O20 U3
Calculated formula	Br F Ge4 K8 O20 U3
Title of publication	Crystal growth of novel 3D skeleton uranyl germanium complexes: influence of synthetic conditions on crystal structures.
Authors of publication	Li, Haijian; Kegler, Philip; Alekseev, Evgeny V.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	7
Pages of publication	2244 - 2257
a	7.3647 ± 0.0003 Å
b	9.7768 ± 0.0006 Å
c	9.9186 ± 0.0005 Å
α	70.779 ± 0.005°
β	89.613 ± 0.004°
γ	87.291 ± 0.004°
Cell volume	673.58 ± 0.06 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1251
Residual factor for significantly intense reflections	0.0757
Weighted residual factors for significantly intense reflections	0.2056
Weighted residual factors for all reflections included in the refinement	0.2193
Goodness-of-fit parameter for all reflections included in the refinement	1.074
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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