Information card for entry 7703371

Structure parameters

• Formula: C5 H12 Cl8 S4 W2
• Calculated formula: C5 H12 Cl8 S4 W2
• Title of publication: Thioether complexes of WSCl₄, WOCl₄ and WSCl₃ and evaluation of thiochloride complexes as CVD precursors for WS₂ thin films.
• Authors of publication: Smith, Danielle E.; Greenacre, Victoria K.; Hector, Andrew L.; Huang, Ruomeng; Levason, William; Reid, Gillian; Robinson, Fred; Thomas, Shibin
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 8
• Pages of publication: 2496 - 2504
• a: 6.6665 ± 0.0002 Å
• b: 11.1479 ± 0.0002 Å
• c: 13.8916 ± 0.0003 Å
• α: 101.979 ± 0.002°
• β: 100.011 ± 0.002°
• γ: 95.717 ± 0.002°
• Cell volume: 984.61 ± 0.04 ų
• Cell temperature: 100.03 ± 0.1 K
• Ambient diffraction temperature: 100.03 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.058
• Residual factor for significantly intense reflections: 0.0495
• Weighted residual factors for significantly intense reflections: 0.1182
• Weighted residual factors for all reflections included in the refinement: 0.1279
• Goodness-of-fit parameter for all reflections included in the refinement: 1.177
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No