Information card for entry 7703377

Structure parameters

• Formula: C4 H10 Cl3 S3 W
• Calculated formula: C4 H10 Cl3 S3 W
• Title of publication: Thioether complexes of WSCl₄, WOCl₄ and WSCl₃ and evaluation of thiochloride complexes as CVD precursors for WS₂ thin films.
• Authors of publication: Smith, Danielle E.; Greenacre, Victoria K.; Hector, Andrew L.; Huang, Ruomeng; Levason, William; Reid, Gillian; Robinson, Fred; Thomas, Shibin
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 8
• Pages of publication: 2496 - 2504
• a: 6.8758 ± 0.0001 Å
• b: 13.2588 ± 0.0002 Å
• c: 12.5782 ± 0.0002 Å
• α: 90°
• β: 94.541 ± 0.002°
• γ: 90°
• Cell volume: 1143.09 ± 0.03 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0432
• Residual factor for significantly intense reflections: 0.0391
• Weighted residual factors for significantly intense reflections: 0.0748
• Weighted residual factors for all reflections included in the refinement: 0.0763
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No