Information card for entry 7703408

Structure parameters

• Formula: C33 H52 Si2 Ti
• Calculated formula: C33 H52 Si2 Ti
• Title of publication: Synthesis of a titanium ethylene complex via C-H-activation and alternative access to Cp₂Ti(η²-Me₃SiC₂SiMe₃).
• Authors of publication: Fischer, Malte; Vincent-Heldt, Lisa; Hillje, Malena; Schmidtmann, Marc; Beckhaus, Ruediger
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 7
• Pages of publication: 2068 - 2072
• a: 11.3854 ± 0.0003 Å
• b: 12.8121 ± 0.0003 Å
• c: 21.3362 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3112.33 ± 0.13 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0205
• Residual factor for significantly intense reflections: 0.0193
• Weighted residual factors for significantly intense reflections: 0.0542
• Weighted residual factors for all reflections included in the refinement: 0.055
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No