Information card for entry 7703417

Structure parameters

• Formula: C32 H29 Cl Co N4 O7
• Calculated formula: C32 H29 Cl Co N4 O7
• Title of publication: Oxidative C-N bond cleavage of (2-pyridylmethyl)amine-based tetradentate supporting ligands in ternary cobalt(ii)-carboxylate complexes.
• Authors of publication: Chakraborty, Biswarup; Ghosh, Ivy; Jana, Rahul Dev; Paine, Tapan Kanti
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 11
• Pages of publication: 3463 - 3472
• a: 10.6498 ± 0.0012 Å
• b: 12.2814 ± 0.0014 Å
• c: 13.1786 ± 0.0016 Å
• α: 75.85 ± 0.005°
• β: 83.335 ± 0.005°
• γ: 66.493 ± 0.005°
• Cell volume: 1532.3 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.053
• Residual factor for significantly intense reflections: 0.0499
• Weighted residual factors for significantly intense reflections: 0.1598
• Weighted residual factors for all reflections included in the refinement: 0.1651
• Goodness-of-fit parameter for all reflections included in the refinement: 1.236
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No