Information card for entry 7703563

Structure parameters

• Formula: C96.75 H127 B2 Br2 Li4 N4 O4
• Calculated formula: C96.7496 H126.999 B2 Br2 Li4 N4 O3.9999
• Title of publication: Alkali metal reduction of 1,3,2-diazaborol and 1,3,2-diazagermol derivatives based on 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene.
• Authors of publication: Lukina, Daria A.; Skatova, Alexandra A.; Lukoyanov, Anton N.; Kozlova, Ekaterina A.; Fedushkin, Igor L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 9
• Pages of publication: 2941 - 2946
• a: 13.2924 ± 0.0004 Å
• b: 14.4434 ± 0.0003 Å
• c: 24.8139 ± 0.0007 Å
• α: 101.192 ± 0.002°
• β: 102.617 ± 0.002°
• γ: 91.829 ± 0.002°
• Cell volume: 4546.7 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0997
• Residual factor for significantly intense reflections: 0.0551
• Weighted residual factors for significantly intense reflections: 0.1285
• Weighted residual factors for all reflections included in the refinement: 0.1456
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No