Information card for entry 7703697

Structure parameters

• Formula: C37 H29 B O3 P2
• Calculated formula: C37 H29 B O3 P2
• Title of publication: The phosphinoboration of acyl chlorides.
• Authors of publication: Murphy, Maia C.; Trofimova, Alina; LaFortune, James H. W.; Vogels, Christopher M.; Geier, Stephen J.; Binder, Justin F.; Macdonald, Charles L. B.; Stephan, Douglas W.; Westcott, Stephen A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 16
• Pages of publication: 5092 - 5099
• a: 10.299 ± 0.004 Å
• b: 10.93 ± 0.003 Å
• c: 14.818 ± 0.005 Å
• α: 76.664 ± 0.012°
• β: 84.069 ± 0.012°
• γ: 68.725 ± 0.012°
• Cell volume: 1512.1 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0912
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for significantly intense reflections: 0.0969
• Weighted residual factors for all reflections included in the refinement: 0.1221
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No