Information card for entry 7703710

Structure parameters

• Formula: C67 H82 B2 F5 Ge2 N6 O
• Calculated formula: C67 H82 B2 F5 Ge2 N6 O
• Title of publication: Reactivity of boraguanidinato germylenes toward carbonyl compounds and isocyanides: C-O, C-F and C-N bond activation.
• Authors of publication: Böserle, Jiří; Jambor, Roman; RůŽička, Aleš; Erben, Milan; Dostál, Libor
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 15
• Pages of publication: 4869 - 4877
• a: 13.2217 ± 0.001 Å
• b: 13.5451 ± 0.0011 Å
• c: 20.1024 ± 0.0015 Å
• α: 78.791 ± 0.002°
• β: 74.532 ± 0.002°
• γ: 66.824 ± 0.002°
• Cell volume: 3173.4 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0512
• Residual factor for significantly intense reflections: 0.0424
• Weighted residual factors for significantly intense reflections: 0.0982
• Weighted residual factors for all reflections included in the refinement: 0.1036
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No