Information card for entry 7703754

Structure parameters

• Formula: C39.25 H38.5 Cl1.5 F6 Fe N3 P Pd Sb
• Calculated formula: C39.25 H38.5 Cl1.5 F6 Fe N3 P Pd Sb
• Title of publication: Synthesis and study of Fe →Pd interactions in unsymmetric Pd(ii) complexes with phosphinoferrocene guanidine ligands.
• Authors of publication: Bárta, Ondřej; Gyepes, Róbert; Císařová, Ivana; Alemayehu, Adam; Štěpnička, Petr
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 14
• Pages of publication: 4225 - 4229
• a: 10.8536 ± 0.0005 Å
• b: 11.6697 ± 0.0005 Å
• c: 17.6614 ± 0.0008 Å
• α: 97.12 ± 0.001°
• β: 106.206 ± 0.001°
• γ: 108.55 ± 0.001°
• Cell volume: 1980.09 ± 0.16 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0249
• Residual factor for significantly intense reflections: 0.0237
• Weighted residual factors for significantly intense reflections: 0.0599
• Weighted residual factors for all reflections included in the refinement: 0.0607
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No