Crystallography Open Database

Information card for entry 7703768

Preview

Coordinates	7703768.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C78 H64 Br4 N4 Ni2 O2
Calculated formula	C78 H64 Br4 N4 Ni2 O2
Title of publication	Systematic studies on dibenzhydryl and pentiptycenyl substituted pyridine-imine nickel(ii) mediated ethylene polymerization.
Authors of publication	Wang, Chaoqun; Zhang, Yuxing; Mu, Hongliang; Jian, Zhongbao
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	15
Pages of publication	4824 - 4833
a	9.5838 ± 0.0006 Å
b	13.0175 ± 0.0009 Å
c	13.8929 ± 0.0009 Å
α	96.049 ± 0.001°
β	91.88 ± 0.001°
γ	107.217 ± 0.001°
Cell volume	1642.61 ± 0.19 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173.01 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0358
Residual factor for significantly intense reflections	0.0284
Weighted residual factors for significantly intense reflections	0.0711
Weighted residual factors for all reflections included in the refinement	0.0756
Goodness-of-fit parameter for all reflections included in the refinement	1.02
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7703768.html