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Information card for entry 7703839
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Coordinates | 7703839.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C52 H38 B F24 N2 Rh S2 Si |
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Calculated formula | C52 H38 B F24 N2 Rh S2 Si |
Title of publication | Si-C(sp<sup>3</sup>) bond activation through oxidative addition at a Rh(i) centre. |
Authors of publication | Azpeitia, S.; Martínez-Martínez, A J; Garralda, M. A.; Weller, A. S.; Huertos, M. A. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2020 |
Journal volume | 49 |
Journal issue | 17 |
Pages of publication | 5416 - 5419 |
a | 13.0258 ± 0.0004 Å |
b | 14.6748 ± 0.0005 Å |
c | 16.5971 ± 0.0006 Å |
α | 64.937 ± 0.003° |
β | 82.448 ± 0.003° |
γ | 74.53 ± 0.003° |
Cell volume | 2769.1 ± 0.18 Å3 |
Cell temperature | 150.01 ± 0.1 K |
Ambient diffraction temperature | 150.01 ± 0.1 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0593 |
Residual factor for significantly intense reflections | 0.0546 |
Weighted residual factors for significantly intense reflections | 0.1486 |
Weighted residual factors for all reflections included in the refinement | 0.1536 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.036 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7703839.html
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