Crystallography Open Database

Information card for entry 7703880

Preview

Coordinates	7703880.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	[Rh(N3Dipp2)(COD)]
Formula	C32 H46 N3 Rh
Calculated formula	C32 H46 N3 Rh
Title of publication	Bulky bis(aryl)triazenides: just aspiring amidinates? A structural and spectroscopic study.
Authors of publication	Gyton, Matthew R.; Leverett, Anthony R.; Cole, Marcus L.; McKay, Alasdair I.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	17
Pages of publication	5653 - 5661
a	17.0526 ± 0.0008 Å
b	8.8969 ± 0.0003 Å
c	18.8292 ± 0.0008 Å
α	90°
β	93.738 ± 0.002°
γ	90°
Cell volume	2850.6 ± 0.2 Å³
Cell temperature	150.15 K
Ambient diffraction temperature	150.15 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0189
Residual factor for significantly intense reflections	0.0186
Weighted residual factors for significantly intense reflections	0.0477
Weighted residual factors for all reflections included in the refinement	0.0479
Goodness-of-fit parameter for all reflections included in the refinement	1.117
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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