Crystallography Open Database

Information card for entry 7703888

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Coordinates	7703888.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	[Na(DME)2(N3Dipp2)]
Formula	C32 H54 N3 Na O4
Calculated formula	C32 H54 N3 Na O4
Title of publication	Bulky bis(aryl)triazenides: just aspiring amidinates? A structural and spectroscopic study.
Authors of publication	Gyton, Matthew R.; Leverett, Anthony R.; Cole, Marcus L.; McKay, Alasdair I.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	17
Pages of publication	5653 - 5661
a	20.0231 ± 0.0015 Å
b	10.9042 ± 0.0008 Å
c	33.135 ± 0.003 Å
α	90°
β	105.34 ± 0.004°
γ	90°
Cell volume	6976.8 ± 1 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	149.99 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.2242
Residual factor for significantly intense reflections	0.078
Weighted residual factors for significantly intense reflections	0.1772
Weighted residual factors for all reflections included in the refinement	0.2454
Goodness-of-fit parameter for all reflections included in the refinement	0.978
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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