Crystallography Open Database

Information card for entry 7703893

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Coordinates	7703893.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	[Tl(N3Dipp2)]2
Formula	C48 H68 N6 Tl2
Calculated formula	C48 H68 N6 Tl2
Title of publication	Bulky bis(aryl)triazenides: just aspiring amidinates? A structural and spectroscopic study.
Authors of publication	Gyton, Matthew R.; Leverett, Anthony R.; Cole, Marcus L.; McKay, Alasdair I.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	17
Pages of publication	5653 - 5661
a	13.5767 ± 0.0005 Å
b	20.2026 ± 0.0007 Å
c	35.6666 ± 0.0011 Å
α	90°
β	90°
γ	90°
Cell volume	9782.8 ± 0.6 Å³
Cell temperature	180 K
Ambient diffraction temperature	180.15 K
Number of distinct elements	4
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0671
Residual factor for significantly intense reflections	0.0379
Weighted residual factors for significantly intense reflections	0.0554
Weighted residual factors for all reflections included in the refinement	0.0615
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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