Information card for entry 7703909

Structure parameters

• Formula: C32 H22 O14 P2 W2
• Calculated formula: C32.0012 H22 O14.0012 P2 W1.9988
• Title of publication: Phosphacycloalkyldiones: synthesis and coordinative behaviour of 6- and 7-member cyclic diketophosphanyls.
• Authors of publication: Pearce, Kyle G.; Simenok, Vladimir; Crossley, Ian R.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 17
• Pages of publication: 5482 - 5492
• a: 11.0044 ± 0.0003 Å
• b: 9.7434 ± 0.0003 Å
• c: 32.7494 ± 0.001 Å
• α: 90°
• β: 91.882 ± 0.003°
• γ: 90°
• Cell volume: 3509.51 ± 0.18 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 10 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0798
• Residual factor for significantly intense reflections: 0.0672
• Weighted residual factors for significantly intense reflections: 0.1603
• Weighted residual factors for all reflections included in the refinement: 0.1672
• Goodness-of-fit parameter for all reflections included in the refinement: 1.15
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No