Information card for entry 7703989

Structure parameters

• Formula: H48 K6 N16 Sn8 Zn
• Calculated formula: H48 K6 N16 Sn8 Zn
• Title of publication: Intermediates and products of the reaction of Zn(ii) organyls with tetrel element Zintl ions: cluster extension versus complexation.
• Authors of publication: Wallach, C.; Mayer, K.; Henneberger, T.; Klein, W.; Fässler, T F
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 19
• Pages of publication: 6191 - 6198
• a: 9.6916 ± 0.0006 Å
• b: 12.2418 ± 0.0007 Å
• c: 18.6684 ± 0.0008 Å
• α: 99.12 ± 0.004°
• β: 90.067 ± 0.004°
• γ: 94.894 ± 0.005°
• Cell volume: 2178.7 ± 0.2 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0494
• Residual factor for significantly intense reflections: 0.0322
• Weighted residual factors for significantly intense reflections: 0.0667
• Weighted residual factors for all reflections included in the refinement: 0.0694
• Goodness-of-fit parameter for all reflections included in the refinement: 0.919
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No