Information card for entry 7703992

Structure parameters

• Formula: C47 H76 K N O8 Zn
• Calculated formula: C47 H76 K N O8 Zn
• Title of publication: Intermediates and products of the reaction of Zn(ii) organyls with tetrel element Zintl ions: cluster extension versus complexation.
• Authors of publication: Wallach, C.; Mayer, K.; Henneberger, T.; Klein, W.; Fässler, T F
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 19
• Pages of publication: 6191 - 6198
• a: 15.757 ± 0.0005 Å
• b: 13.1722 ± 0.0005 Å
• c: 23.6712 ± 0.0008 Å
• α: 90°
• β: 94.486 ± 0.003°
• γ: 90°
• Cell volume: 4898 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.095
• Residual factor for significantly intense reflections: 0.0455
• Weighted residual factors for significantly intense reflections: 0.1018
• Weighted residual factors for all reflections included in the refinement: 0.1107
• Goodness-of-fit parameter for all reflections included in the refinement: 0.84
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No