Information card for entry 7703994

Structure parameters

• Formula: C32 H99 K2 N13 O12 Zn5
• Calculated formula: C32 H99 K2 N13 O12 Zn5
• Title of publication: Intermediates and products of the reaction of Zn(ii) organyls with tetrel element Zintl ions: cluster extension versus complexation.
• Authors of publication: Wallach, C.; Mayer, K.; Henneberger, T.; Klein, W.; Fässler, T F
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 19
• Pages of publication: 6191 - 6198
• a: 11.554 ± 0.002 Å
• b: 14.14 ± 0.003 Å
• c: 18.988 ± 0.004 Å
• α: 89.02 ± 0.03°
• β: 77.37 ± 0.03°
• γ: 87.11 ± 0.03°
• Cell volume: 3023.2 ± 1.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.034
• Residual factor for significantly intense reflections: 0.0267
• Weighted residual factors for significantly intense reflections: 0.0613
• Weighted residual factors for all reflections included in the refinement: 0.0668
• Goodness-of-fit parameter for all reflections included in the refinement: 1.104
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No