Information card for entry 7704011

Structure parameters

• Formula: C16 Al F36 K O4
• Calculated formula: C16 Al F36 K O4
• Title of publication: Building blocks for the chemistry of perfluorinated alkoxyaluminates [Al{OC(CF₃)₃}₄]^-: simplified preparation and characterization of Li⁺-Cs⁺, Ag⁺, NH₄⁺, N₂H₅⁺ and N₂H₇⁺ salts.
• Authors of publication: Malinowski, Przemysław J; Jaroń, Tomasz; Domańska, Małgorzata; Slattery, John M.; Schmitt, Manuel; Krossing, Ingo
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 23
• Pages of publication: 7766 - 7773
• a: 23.8816 ± 0.0011 Å
• b: 12.9259 ± 0.0006 Å
• c: 20.6284 ± 0.001 Å
• α: 90°
• β: 115.546 ± 0.002°
• γ: 90°
• Cell volume: 5745.3 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0389
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for significantly intense reflections: 0.082
• Weighted residual factors for all reflections included in the refinement: 0.0847
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No