Information card for entry 7704081

Structure parameters

• Formula: B11 Ba3 H5 O23 Pb
• Calculated formula: B11 Ba3 O23 Pb
• Title of publication: High-temperature, high-pressure hydrothermal synthesis, crystal structure, and infrared and NMR spectroscopy of a barium lead borate with a 2D layer structure: [Ba₃Pb(H₂O)][B₁₁O₁₉(OH)₃].
• Authors of publication: Kuo, Yu-Chen; Liu, Hsin-Kuan; Wang, Sue-Lein; Lii, Kwang-Hwa
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 19
• Pages of publication: 6220 - 6226
• a: 6.658 ± 0.0002 Å
• b: 30.3359 ± 0.0008 Å
• c: 8.7411 ± 0.0002 Å
• α: 90°
• β: 90.952 ± 0.001°
• γ: 90°
• Cell volume: 1765.25 ± 0.08 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0368
• Residual factor for significantly intense reflections: 0.0362
• Weighted residual factors for significantly intense reflections: 0.0894
• Weighted residual factors for all reflections included in the refinement: 0.0899
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No