Information card for entry 7704152

Structure parameters

• Formula: H39 K3 Nb14 O58 Si
• Calculated formula: K3 Nb14 O58 Si
• Title of publication: Syntheses, characterization and properties of two new dodeca-niobates presenting unprecedented features.
• Authors of publication: Zhang, Ting-Ting; Lin, Po-Han; Yu, Gui-Yang; Zhang, Xiao; Cui, Xiao-Bing
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 19
• Pages of publication: 6495 - 6503
• a: 10.8913 ± 0.0008 Å
• b: 11.6608 ± 0.0008 Å
• c: 19.6414 ± 0.0015 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2494.5 ± 0.3 ų
• Cell temperature: 301 ± 2 K
• Ambient diffraction temperature: 301 ± 2 K
• Number of distinct elements: 5
• Space group number: 23
• Hermann-Mauguin space group symbol: I 2 2 2
• Hall space group symbol: I 2 2
• Residual factor for all reflections: 0.0845
• Residual factor for significantly intense reflections: 0.0758
• Weighted residual factors for significantly intense reflections: 0.2183
• Weighted residual factors for all reflections included in the refinement: 0.229
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No