Crystallography Open Database

Information card for entry 7704180

Preview

Coordinates	7704180.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H60 Li2 Mg N4 O4
Calculated formula	C34 H60 Li2 Mg N4 O4
Title of publication	Alkali-metal organomagnesiate complexes as catalysts for highly chemoselective crossed-Tishchenko reactions.
Authors of publication	Guo, Zhiqiang; Pang, Tengfei; Wang, Yakong; Zhang, Yongbin; Wei, Xuehong
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	19
Pages of publication	6418 - 6424
a	22.586 ± 0.002 Å
b	11.7778 ± 0.0012 Å
c	17.703 ± 0.003 Å
α	90°
β	126.618 ± 0.002°
γ	90°
Cell volume	3779.8 ± 0.8 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1635
Residual factor for significantly intense reflections	0.0795
Weighted residual factors for significantly intense reflections	0.1336
Weighted residual factors for all reflections included in the refinement	0.1826
Goodness-of-fit parameter for all reflections included in the refinement	0.989
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7704180.html