Crystallography Open Database

Information card for entry 7704182

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Coordinates	7704182.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H77 Mg2 N8 Na2
Calculated formula	C38 H77 Mg2 N8 Na2
Title of publication	Alkali-metal organomagnesiate complexes as catalysts for highly chemoselective crossed-Tishchenko reactions.
Authors of publication	Guo, Zhiqiang; Pang, Tengfei; Wang, Yakong; Zhang, Yongbin; Wei, Xuehong
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	19
Pages of publication	6418 - 6424
a	18.5707 ± 0.0007 Å
b	17.223 ± 0.0006 Å
c	15.7369 ± 0.0006 Å
α	90°
β	112.561 ± 0.001°
γ	90°
Cell volume	4648.1 ± 0.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.094
Residual factor for significantly intense reflections	0.0704
Weighted residual factors for significantly intense reflections	0.1882
Weighted residual factors for all reflections included in the refinement	0.2121
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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