Crystallography Open Database

Information card for entry 7704184

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Coordinates	7704184.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H66 Mg2 N4 Na2 O2
Calculated formula	C34 H66 Mg2 N4 Na2 O2
Title of publication	Alkali-metal organomagnesiate complexes as catalysts for highly chemoselective crossed-Tishchenko reactions.
Authors of publication	Guo, Zhiqiang; Pang, Tengfei; Wang, Yakong; Zhang, Yongbin; Wei, Xuehong
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	19
Pages of publication	6418 - 6424
a	17.2336 ± 0.0006 Å
b	19.0795 ± 0.0006 Å
c	24.5532 ± 0.0008 Å
α	90°
β	90°
γ	90°
Cell volume	8073.3 ± 0.5 Å³
Cell temperature	136 ± 2 K
Ambient diffraction temperature	135.93 K
Number of distinct elements	6
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0666
Residual factor for significantly intense reflections	0.0561
Weighted residual factors for significantly intense reflections	0.147
Weighted residual factors for all reflections included in the refinement	0.1617
Goodness-of-fit parameter for all reflections included in the refinement	1.062
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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