Information card for entry 7704218

Structure parameters

• Chemical name: [La(Htp)2(BH4)2K(DME)2]2
• Formula: C64 H136 B4 K2 La2 O8 P4
• Calculated formula: C64 H136 B4 K2 La2 O8 P4
• Title of publication: Synthesis and characterisation of light lanthanide bis-phospholyl borohydride complexes.
• Authors of publication: Liu, Jingjing; Nodaraki, Lydia E.; Cobb, Philip J.; Giansiracusa, Marcus J.; Ortu, Fabrizio; Tuna, Floriana; Mills, David P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 19
• Pages of publication: 6504 - 6511
• a: 10.679 ± 0.0002 Å
• b: 21.0788 ± 0.0004 Å
• c: 18.755 ± 0.0005 Å
• α: 90°
• β: 98.041 ± 0.002°
• γ: 90°
• Cell volume: 4180.25 ± 0.16 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0392
• Residual factor for significantly intense reflections: 0.0278
• Weighted residual factors for significantly intense reflections: 0.0579
• Weighted residual factors for all reflections included in the refinement: 0.0611
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No