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Information card for entry 7704224
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Coordinates | 7704224.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | (MeClamp)Os |
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Chemical name | [Tris(2-(3',5'-di-tert-butyl-2'-oxyphenyl)amido-4- methylphenyl)amine]osmium(VI) |
Formula | C63 H78 N4 O3 Os |
Calculated formula | C63 H78 N4 O3 Os |
Title of publication | Highly covalent metal-ligand π bonding in chelated bis- and tris(iminoxolene) complexes of osmium and ruthenium. |
Authors of publication | Gianino, Jacqueline; Brown, Seth N. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2020 |
Journal volume | 49 |
Journal issue | 21 |
Pages of publication | 7015 - 7027 |
a | 12.2048 ± 0.0011 Å |
b | 28.05 ± 0.003 Å |
c | 17.3586 ± 0.0016 Å |
α | 90° |
β | 92.9257 ± 0.0013° |
γ | 90° |
Cell volume | 5934.9 ± 1 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0472 |
Residual factor for significantly intense reflections | 0.0297 |
Weighted residual factors for significantly intense reflections | 0.0536 |
Weighted residual factors for all reflections included in the refinement | 0.0573 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.002 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7704224.html
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