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Information card for entry 7704307
Preview
Coordinates | 7704307.cif |
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Original paper (by DOI) | HTML |
Formula | C54.22 H84.22 Br Ge N2 O4 S2 Si4 |
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Calculated formula | C54.222 H84.222 Br Ge N2 O4 S2 Si4 |
Title of publication | 1,2-Insertion reactions of alkynes into Ge-C bonds of arylbromogermylene. |
Authors of publication | Sugahara, Tomohiro; Espinosa Ferao, Arturo; Rey Planells, Alicia; Guo, Jing-Dong; Aoyama, Shin; Igawa, Kazunobu; Tomooka, Katsuhiko; Sasamori, Takahiro; Hashizume, Daisuke; Nagase, Shigeru; Tokitoh, Norihiro |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2020 |
Journal volume | 49 |
Journal issue | 21 |
Pages of publication | 7189 - 7196 |
a | 11.8162 ± 0.0002 Å |
b | 12.9307 ± 0.0003 Å |
c | 23.7235 ± 0.0006 Å |
α | 74.247 ± 0.002° |
β | 88.954 ± 0.002° |
γ | 65.242 ± 0.002° |
Cell volume | 3149.01 ± 0.14 Å3 |
Cell temperature | 103 ± 2 K |
Ambient diffraction temperature | 103.15 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0943 |
Residual factor for significantly intense reflections | 0.0674 |
Weighted residual factors for significantly intense reflections | 0.1639 |
Weighted residual factors for all reflections included in the refinement | 0.1788 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.087 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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