Information card for entry 7704359

Structure parameters

• Formula: C31.5 H31.5 B0.5 Cl0 F12 O P Ru0.5
• Calculated formula: C31.5 H31.5 B0.5 F12 O P Ru0.5
• Title of publication: Conformation controlled stepwise hydride shuffling from the metal to the ligand backbone.
• Authors of publication: Wiedmaier, Nicholas R.; Speth, Hansjörg; Leistikow, Georg; Eichele, Klaus; Schubert, Hartmut; Mayer, Hermann A.; Wesemann, Lars
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 21
• Pages of publication: 7218 - 7227
• a: 12.9706 ± 0.0003 Å
• b: 16.5597 ± 0.0003 Å
• c: 31.8663 ± 0.0007 Å
• α: 90°
• β: 99.524 ± 0.001°
• γ: 90°
• Cell volume: 6750.2 ± 0.2 ų
• Cell temperature: 99 ± 2 K
• Ambient diffraction temperature: 99 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0532
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for significantly intense reflections: 0.1026
• Weighted residual factors for all reflections included in the refinement: 0.1098
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No