Information card for entry 7704516

Structure parameters

• Formula: C68 H87.86 Cl3.92 Hf Mo2 N6 Na2 O24 P12
• Calculated formula: C68 H87.868 Cl3.92 Hf Mo2 N6 Na2 O24 P12
• Title of publication: 1,3,4-Azadiphospholides as building blocks for scorpionate and bidentate ligands in multinuclear complexes.
• Authors of publication: Suter, Riccardo; Wagner, Mona; Querci, Lorenzo; Conti, Riccardo; Benkő, Zoltán; Grützmacher, Hansjörg
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 24
• Pages of publication: 8201 - 8208
• a: 13.1135 ± 0.0003 Å
• b: 13.1212 ± 0.0004 Å
• c: 16.9409 ± 0.0004 Å
• α: 83.345 ± 0.002°
• β: 68.758 ± 0.002°
• γ: 60.501 ± 0.003°
• Cell volume: 2357.65 ± 0.13 ų
• Cell temperature: 104 ± 2 K
• Ambient diffraction temperature: 104 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0253
• Residual factor for significantly intense reflections: 0.023
• Weighted residual factors for significantly intense reflections: 0.0529
• Weighted residual factors for all reflections included in the refinement: 0.0538
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No