Information card for entry 7704539

Structure parameters

• Formula: C36 H58 Ge N3 Ni P
• Calculated formula: C36 H58 Ge N3 Ni P
• SMILES: CC(C)(C)N1C(c2ccccc2)=[N](C(C)(C)C)[Ge]21n1cccc1C[P](C(C)(C)C)(C(C)(C)C)[Ni]1342[CH]2=[CH]1CC[CH]3=[CH]4CC2
• Title of publication: Phosphane-functionalized heavier tetrylenes: synthesis of silylene- and germylene-decorated phosphanes and their reactions with Group 10 metal complexes.
• Authors of publication: Cabeza, Javier A.; García-Álvarez, Pablo; Laglera-Gándara, Carlos J; Pérez-Carreño, Enrique
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 24
• Pages of publication: 8331 - 8339
• a: 20.5915 ± 0.0011 Å
• b: 8.8479 ± 0.0003 Å
• c: 20.8528 ± 0.0008 Å
• α: 90°
• β: 109.118 ± 0.005°
• γ: 90°
• Cell volume: 3589.7 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1865
• Residual factor for significantly intense reflections: 0.0747
• Weighted residual factors for significantly intense reflections: 0.0798
• Weighted residual factors for all reflections included in the refinement: 0.1084
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No