Crystallography Open Database

Information card for entry 7704661

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Coordinates	7704661.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H74 N4 Si5
Calculated formula	C40 H74 N4 Si5
Title of publication	Probing the non-innocent nature of an amino-functionalised β-diketiminate ligand in silylene/iminosilane systems.
Authors of publication	Do, Dinh Cao Huan; Vasko, Petra; Fuentes, M Ángeles; Hicks, Jamie; Aldridge, Simon
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	25
Pages of publication	8701 - 8709
a	19.7161 ± 0.0005 Å
b	10.7126 ± 0.0002 Å
c	22.358 ± 0.0005 Å
α	90°
β	98.43 ± 0.002°
γ	90°
Cell volume	4671.23 ± 0.18 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0454
Residual factor for significantly intense reflections	0.0351
Weighted residual factors for significantly intense reflections	0.0887
Weighted residual factors for all reflections included in the refinement	0.0966
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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