Information card for entry 7704671

Structure parameters

• Formula: C165 H167 B4 Cl9 Co4 N40 O2
• Calculated formula: C165 H167 B4 Cl9 Co4 N40 O2
• Title of publication: Two azido-bridged [2×2] cobalt(ii) grids featuring single-molecule magnet behaviour.
• Authors of publication: Guo, Zhilin; Deng, Yi-Fei; Zhang, Yipei; Pikramenou, Zoe; Zhang, Yuan-Zhu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2020
• Journal volume: 49
• Journal issue: 27
• Pages of publication: 9218 - 9222
• a: 17.9901 ± 0.0018 Å
• b: 19.0049 ± 0.0019 Å
• c: 28.923 ± 0.003 Å
• α: 89.17 ± 0.005°
• β: 72.435 ± 0.005°
• γ: 62.773 ± 0.005°
• Cell volume: 8293.6 ± 1.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100.02 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0664
• Residual factor for significantly intense reflections: 0.0506
• Weighted residual factors for significantly intense reflections: 0.1218
• Weighted residual factors for all reflections included in the refinement: 0.1315
• Goodness-of-fit parameter for all reflections included in the refinement: 1.074
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No